ReactIR Continuous Flow Analyzer
FTIR Analyzer for Continuous Flow Chemistry Applications
Researchers are increasingly using continuous flow chemistry to develop new reactions and processes with increased specificity, yield and product quality. Optimization of this work is often challenging as offline analytical techniques, such as High-Performance Liquid Chromatography (HPLC), cannot provide fast enough information to optimize the reaction in real time. A dedicated ReactIR Fourier Transform Infrared Spectroscopy (FTIR) instrument for in-situ, real-time monitoring of continuous flow chemistry, enables researchers to save valuable time and materials when screening and optimizing their reactions.
Examples of ReactIR value in continuous flow chemistry include:
- Oxazole formation
- Fluorination reaction
- Accurate control of reagent addition in multi-step segmented flow processes
- Analysis of a continuous process for alkene ozonolysis
Small and Lightweight
The streamlined profile fits easily into physically constrained areas, meaning the instrument can be placed along the reaction sequence to monitor where needed.
No Liquid-Nitrogen Required
Infrared measurements can be made continually and unattended for as long as necessary to accommodate a synthesis.
iC IR 7 Software
Set up and monitoring trends is straightforward and intuitive. Data from the ReactIR 702L can be integrated with control systems to allow for proactive execution of the chemistry.
Specifications
Specifications - ReactIR Continuous Flow Analyzer
| For Use In | Laboratory |
| Software | iC IR |
| Detector | TE MCT |
| Optical Range (Base Unit) | 4000 - 800 cm-1 |
| Purge Requirement | No |
| Resolution | 4 cm -1 maximum |
| Communication | USB |
| Probe Optical Window | 4000 - 650cm-1 (Micro Flow Cell) 4000 – 650 cm-1 (Sentinel) 2500 – 650 cm-1 maximum (Fiber Probe) |
| Probe Pressure (Maximum) | 69bar (6.3 & 9.5mm Fiber Probe) 206bar (Sentinel) 35bar (Micro Flow Cell) |
| Weight | 9.2 lb (4.2 kg) |
| Probe Temperature (Maximum) | 180°C (Fiber Probe) 60°C (Micro Flow Cell) 300°C (Sentinel) |
| Wetted Materials | Diamond or Silicon Alloy C-22 Gold or PTFE |
| Probe pH Range | 1 – 9 (Silicon) 1 – 14 (Diamond) |
| Dimensions (HxWxD) | 4 in x 8.1 in x 9.2 in (100 mm x 206 mm x 234 mm) |
| Laser Safety Certification | IEC 60825 (CE), 21 CFR 1040 (US) |
| Safety Certification | NRTL/C: UL 61010-1, CSA 22.2 No. 61010-1, EN 61326 CE: EN/IEC 61010-1:2012, IEC 61326 |
Documentation
Data Sheets
ReactIR in-situ sampling technology assures usability in a wide range of batch and continuous reaction conditions.
Use spectroscopic data to increase chemical understanding and knowledge of the chemical process and associated critical parameters.
Validate ReactIR wavenumber accuracy and calibrate to a Polystyrene standard certified by the National Institute of Standards and Technology (NIST) fo...
Applications
Continuous flow chemistry opens options with exothermic synthetic steps that are not possible in batch reactors, and new developments in flow reactor...
Chemical synthesis occurs when two or more molecules are combined to form a product molecule that possesses specific properties. There are numerous ex...
Software
iC IR is used by chemists and engineers to gain important insight into reaction initiation, endpoint, mechanism, pathway, and kinetics.
